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Electrochemical analysis of metal oxides. Electrochemical treatment of liquid wastes. This activity consists of five major tasks: 1 evaluation of different electrochemical reactors for the destruction and removal of hazardous waste components, 2 development and validation of engineering process models, 3 radioactive laboratory-scale tests, 4 demonstration of the technology in an engineering-scale size reactor, and 5 analysis and evaluation of testing data.

The development program team is comprised of individuals from federal, academic, and private industry. Work is being carried out in DOE, academic, and private industrial laboratories. Cyclic voltammetry, potential linear V and chronocuolometry methods were carried out to gain electrochemical behavior of glycerol at a gold electrode.

Potassium hydroxide and sulfuric acid were chosen to be the electrolyte for the electro- oxidation of this organic compound. Besides gold plate electrode, gold composite electrode Au-PVC was also used as the working electrode. The Au-PVC composite electrode was characterized by Scanning Electron Microscopy SEM to determine its morphological aspects before and after used in electrochemical oxidation of glycerol.

In alkaline solution, the adsorption of hydroxide species onto the surface of both gold plate and composite Au-PVC electrodes occurs at potential around mV vs SCE. However, at gold plate electrode, there was a small, broad peak before the drastic escalation of current densities which indicates the charge transfer of the chemisorbed OH - anion.

In acidic media, the gold oxide was formed after potential 1. From the cyclic voltammogram glycerol undergo oxidation twice in potassium hydroxide at gold plate and Au-PVC composite electrodes, while in sulfuric acid, oxidation reaction happened once for glycerol on the gold plate electrode. Overall, electrochemical oxidation of glycerol was more effective in alkaline media. Tafel graph which plotted from potential linear V method shows that Au-PVC composite electrode is better than gold plate electrode for the electro- oxidation of glycerol in alkaline solution.

Electrochemical oxidation of glycerol products as analyzed by Gas Chromatography-Mass Spectrometry GC-MS produced several carboxylic acids and phenolic compounds. Electrochemical catalytic treatment of phenol wastewater. The slurry bed catalytic treatment of contaminated water appears to be a promising alternative for the oxidation of aqueous organic pollutants.

In this paper, the electrochemical oxidation of phenol in synthetic wastewater catalyzed by ferric sulfate and potassium permanganate adsorbed onto active bentonite in slurry bed electrolytic reactor with graphite electrode has been investigated. In order to determine the optimum operating condition, the orthogonal experiments were devised and the results revealed that the system of ferric sulfate, potassium permanganate and active bentonite showed a high catalytic efficiency on the process of electrochemical oxidation phenol in initial pH 5.

When the initial concentration of phenol was 0. According to the experimental results, a possible mechanism of catalytic degradation of phenol was proposed. Environmental estimation was also done and the results showed that the treated wastewater have little impact on plant growth and could totally be applied to irrigation. Ma Hongzhu, E-mail: hzmachem snnu. Removal of pharmaceuticals from wastewater by electrochemical oxidation using cylindrical flow reactor and optimization of treatment conditions.

This paper examines the use of electrooxidation for treatment of wastewater obtained from a pharmaceutical industry. The wastewater primarily contained Gentamicin and Dexamethasone. By cyclic voltammetric CV analysis, the optimum condition for maximum redox reaction was determined. The efficiency of chemical oxygen demand COD reduction and power consumption were studied for different operating conditions. From the results it was observed that maximum COD reduction of about FT-IR spectra studies showed that during electrooxidation, the intensities of characteristic functional groups such as N-H, O-H were reduced and some new peaks also started to appear.

Probable theory, reaction mechanism and modeling were proposed for the oxidation of pharmaceutical effluent. The experimental results demonstrated that electrooxidation treatment was very effective and capable of elevating the quality of treated wastewater to the reuse standard prescribed for pharmaceutical industries. This technology targets the 1 destruction of nitrates, nitrites and organic compounds; 2 removal of radionuclides; and 3 removal of RCRA metals.

The development program consists of five major tasks: 1 evaluation of electrochemical reactors for the destruction and removal of hazardous waste components, 2 development and validation of engineering process models, 3 radioactive laboratory-scale tests, 4 demonstration of the technology in an engineering-scale reactor, and 5 analysis and evaluation of test data.

The development program team is comprised of individuals from national laboratories, academic institutions, and private industry. Possible benefits of this technology include: 1 improved radionuclide separation as a result of the removal of organic complexants, 2 reduction in the concentrations of hazardous and radioactive species in the waste e.

A high-performance flexible fibre-shaped electrochemical capacitor based on electrochemically reduced graphene oxide. A fibre-shaped solid electrochemical capacitor based on electrochemically reduced graphene oxide has been fabricated, exhibiting high specific capacitance and rate capability, long cycling life and attractive flexibility.

The electrochemical oxidation using boron-doped diamond electrodes processes was carried out using three current density values: 3. An optimal degradation condition for the ozonation treatment is at alkaline pH, while the electrochemical treatment works better at acidic pH. The electrochemical process is twice better compared with ozonation. Obtention of superconductivity by room temperature electrochemical oxidation of La2CuO4.

The undoped oxide La2CuO4 has required traditionally synthesis under high pressure of oxygen and high temperatures to incorporate excess oxygen into its structure and become a superconductor. The electrochemical oxidation of this same oxide at room temperature and pressure constitutes a striking example of the use of an alternative driving force for the oxidation of oxides to become superconductors.

Electrochemical treatment of oxides has been frequently applied to their reduction with cationic intercalation. Oxidations of these solid with the concomitant intercalation of anions into their lattice shows also great promises. The paper reports recent results in the electrochemical oxidation of La2CuO4 and other cuprates, showing also the important role of post- oxidation thermal treatments on the properties of the resulting solids.

Electrochemical oxidation and detection of sodium urate in alkaline Electrochemical behaviour of copper oxides electrode in the presence of sodium urate was investigated. The correlation between the anodic oxidation and the amperometric detection of sodium urate in the alkaline medium on copper oxides electrode was analysed by cyclic voltammetry CV and electrochemical Synthesis of magnetite nanoparticles using electrochemical oxidation. Full Text Available The monodisperse magnetite nanoparticles are promising for use in the biomedical industry for targeted drug delivery, cell separation and biochemical products, Magnetic Resonance Imaging, immunological studies, etc.

Biological and medical purposes require high purity magnetite nanoparticles. Electrochemical methods of producing nanoparticles of magnetite acquire significant spread. The kinetics of electrochemical processes are a function of a larger number of parameters than the kinetics of conventional chemical reaction, thus electrochemical reactions can be thinner and more completely adjusted to give a predetermined size nanoparticles.

In the kinetics of the electrochemical oxidation and reduction the important role is played by the nature of the electrode. In many industrial processes, it is advisable to use lead dioxide anodes with titanium current lead. Saturation magnetization was evaluated by the magnetization curve, for the measured sample in the field with strength. For given electrolytes, different behaviors of anodic aluminum oxide AAO and anodic titanium oxide ATO during electrochemical thinning are explained by ionic and electronic current modes.

Branched structures are unavoidably created in AAO since the switch of ionic to electronic current is slow, whereas the barrier oxide in ATO is thinned without formation of the branched structures. In addition, pore opening can be possible in ATO if chemical etching is performed after the thinning process. The thinning was optimized for complete pore opening in ATO and potential-current behavior is interpreted in terms of ionic current-electronic current switching.

Toxicological characterization was conducted on human lymphocytes using a battery of bioassays. A combined electrochemical treatment and posttreatment with ozone and UV light decreased the level of all physicochemical and radiological parameters below the regulated values. Consequently, the purified sample was neither cytotoxic nor genotoxic, indicating that the presented method could be used for the improvement of water quality from the sites highly contaminated with the mixture of heavy metals and radionuclides.

Spectro- electrochemical and DFT study of tenoxicam metabolites formed by electrochemical oxidation. From these studies, new insights on the nature of the ampholitic species involved during tenoxicam's deprotonation in aqueous solution are presented; see scheme A. Moreover, it is shown that, after the analysis of two different reaction schemes that involve up to 10 different molecules and 12 reaction paths, the electrochemical oxidation of tenoxicam, yields two non-electroactive products that are predominately formed by its fragmentation, after the loss of two electrons.

The nature of these fragments was further confirmed by a chromatography study. New electrochemical and photochemical systems for water and wastewater treatment. With the increasing pressure on a more effective use of water resources, the development of appropriate water treatment technologies become more and more important. Photochemical and electrochemical oxidation processes have been proposed in recent years as an attractive alternative for the treatment of contaminated water containing anthropogenic substances hardly biodegradable as well as to purify and disinfect drinking waters.

The aim of this paper is to present some of our last results demonstrating that electrochemical , photochemical, and the coupling of these processes with biological systems are very promising alternatives for the improvement of the water quality. Both strategies resulted in a successful degradation of 5 PAHs to fulfil the discharge limit on 0. The intermixing-with- oxidant approach can also be applied as a method to address the actual sediment matrix PAHs are hydrophobic compounds and their persistence The proof-of-concept study was conducted both by a direct treatment approach and an intermixing-with- oxidant approach, where the contaminated water was intermixed in different ratios with an electrochemically This sensitivity is found to depend on the state of oxidation of the iridium oxide film; for a higher state of oxidation or more of the oxide in the high.

Diversity in electrochemical oxidation of dihydroxybenzenes in the An interesting diversity in the mechanisms has been observed in electrochemical oxidation Electrochemical treatment of mixed hazardous and radioactive wastes. Electrochemical treatment technologies for mixed hazardous waste are currently under development at Los Alamos National Laboratory. For a mixed waste containing toxic components such as heavy metals and cyanides in addition to a radioactive component, the toxic components can be removed or destroyed by electrochemical technologies allowing for recovery of the radioactive component prior to disposal of the solution.

Mixed wastes with an organic component can be treated by oxidizing the organic compound to carbon dioxide and then recovering the radioactive component. The oxidation can be done directly at the anode or indirectly using an electron transfer mediator. Electrochemical treatment of tannery wastewater using DSA electrodes.

In this work we studied the electrochemical treatment of a tannery wastewater using dimensionally stable anodes DSA containing tin, iridium, ruthenium, and titanium. The electrodes were prepared by thermal decomposition of the polymeric precursors. The electrolyses were performed under galvanostatic conditions, at room temperature. Effects of the oxide composition, current density, and effluent conductivity were investigated, and the current efficiency was calculated as a function of the time for the performed electrolyses.

Results showed that all the studied electrodes led to a decrease in the content of both total phenolic compounds and total organic carbon TOC , as well as lower absorbance in the UV-vis region. Toxicity tests using Daphnia similis demonstrated that the electrochemical treatment reduced the wastewater toxicity. The use of DSA type electrodes in the electrochemical treatment of tannery wastewater proved to be useful since it can promote a decrease in total phenolic compounds, TOC, absorbance, and toxicity.

Full Text Available The textile industry uses the electrochemical techniques both in textile processes such as manufacturing fibers, dyeing processes, and decolorizing fabrics and in wastewaters treatments color removal. Electrochemical reduction reactions are mostly used in sulfur and vat dyeing, but in some cases, they are applied to effluents discoloration. However, the main applications of electrochemical treatments in the textile sector are based on oxidation reactions.

Most of electrochemical oxidation processes involve indirect reactions which imply the generation of hypochlorite or hydroxyl radical in situ. These electrogenerated species are able to bleach indigo-dyed denim fabrics and to degrade dyes in wastewater in order to achieve the effluent color removal.

The aim of this paper is to review the electrochemical techniques applied to textile industry. In particular, they are an efficient method to remove color of textile effluents. The reuse of the discolored effluent is possible, which implies an important saving of salt and water i. The electrochemical biosensing efficiency of uric acid UA detection on an electrochemically reduced graphene oxide ERGO -decorated electrode surface was studied by using various amine linkers used to immobilize ERGO.

The amine linkers aminoethylphenyldiazonium , 2,2'- ethylenedioxy bis ethylamine , 3-aminopro-pyltriethoxysilane, and polyethyleneimine were coated on indium-tin- oxide electrode surfaces through chemical or electrochemical deposition methods.

ERGO-decorated surfaces were prepared by the electrochemical reduction of graphene oxide GO , which was immobilized on the amine-coated electrode surfaces through the electrostatic interaction between GO and the ammonium ion of the linker on the surface. We monitored the sensing results of electrochemical UA detection with differential pulse voltammetry.

Among the different amines tested, 3-aminopropyltriethoxysilane provided the best biosensing performance in terms of sensitivity and reproducibility. Mediated electrochemical oxidation of mixed wastes. Tests were performed with non-radioactive surrogate materials: Trimsol for contaminated cutting oils, and reagent-grade cellulose for contaminated cellulosic wastes. Operating and system parameters that were studied were: use of a silver-nitric acid versus a cobalt-sulfuric acid system, effect of electrolyte temperature, effect of acid concentration, and effect of current density.

Electrochemical reduction of cerium oxide into metal. The Fray Farthing and Chen FFC and Ono and Suzuki OS processes were developed for the reduction of titanium oxide to titanium metal by electrolysis in high temperature molten alkali chloride salts. Present work clarifies, by electro-analytical techniques, the reduction pathway leading to the metal. Corrosion- electrochemical characteristics of oxide -carbide and oxide -nitride coatings formed by electrolytic plasma.

The composition, structure, microhardness and corrosion- electrochemical properties of oxide -carbide and oxide -nitride coatings on titanium in 5n H 2 SO 4 , 50 deg, produced by the method of chemical-heat treatment in electrolytic plasma, containing saturation components of nitrogen and carbon, were investigated. It is shown that the coatings produced have increased hardness, possess high corrosion resistance in sulfuric acid solution at increased temperature, as to their electrochemcial behaviour they are similar to titanium carbide and nitride respectively.

It is shown that high corrosion resistance is ensured by electrochemical mechanism of the oxide -carbide and oxide -nitride coating protection. Innovative oxide materials for electrochemical energy conversion and oxygen separation. Ion-conducting solid metal oxides are widely used in high-temperature electrochemical devices for energy conversion and oxygen separation.

However, liquid metal oxides possessing unique electrochemical properties still remain of limited use. The review demonstrates the potential for practical applications of molten oxides. The transport properties of molten oxide materials are discussed. The emphasis is placed on the chemical diffusion of oxygen in the molten oxide membrane materials for electrochemical energy conversion and oxygen separation.

The thermodynamics of these materials is considered. The dynamic polymer chain model developed to describe the oxygen ion transport in molten oxides is discussed. Prospects for further research into molten oxide materials are outlined. The bibliography includes references. Selective oxidation of organic compounds represents a significant challenge for chemical transformations.

Electrochemical activation of nitroxyls is also well known and offers an appealing alternative to the use of chemical co- oxidants. However, academic and industrial organic synthetic communities have not widely adopted electrochemical methods. Nitroxyl catalysts facilitate effective and selective oxidation of alcohols and aldehydes to ketones and carboxylic acids.

Selective benzylic, allylic, and alpha-heteroatom C-H abstraction can also be achieved with nitroxyls and provides access to oxygenated products when used in combination with molecular oxygen as a radical trap. This thesis reports various chemical and electrochemical oxidation methods that were developed using nitroxyl mediators. Chapter 4 highlights the electrochemical activation of various nitroxyls and reports an in-depth study on electrochemical alcohol oxidation and compares the reactivity of nitroxyls under electrochemical or chemical activation.

N-oxyls can also participate in selective C-H abstraction, and Chapter 5 reports the chemical and electrochemical activation of N-oxyls for radical-mediated C-H oxygenation of hetero arylmethanes. For these electrochemical transformations, the development of.

Electrochemical activity of heavy metal oxides in the process of Feb 2, Electrochemical activity of heavy metal oxides in the process of chloride induced Kinetic study on electrochemical oxidation of catechols in the The electrogenerated This behavior is related to the AAS in acetylene-air flame emission mode. Electrochemical promotion of sulfur dioxide catalytic oxidation. It has been shown that there are two negative potential promotion areas with maximum effects at approximately Therefore the promotion effects at negative polarization are completely non-Faradaic.

The effect at This has been ascribed to a destruction of the vanadium polymeric chains Cuprous oxide thin films grown by hydrothermal electrochemical deposition technique. X-ray diffraction studies reveal the formation of cubic cuprous oxide films in different preferred orientations depending upon the deposition technique used. Film growth, uniformity, grain size, optical band gap and photoelectrochemical response were found to improve in the hydrothermal electrochemical deposition technique.

Electrochemical and partial oxidation of methane. Hydrogen has been the most common fuel used for the fuel cell research but there remains challenging technological hurdles and storage issues with hydrogen fuel. The direct electrochemical oxidation of CH4 a major component of natural gas in a solid oxide fuel cell SOFC to generate electricity has a potential of commercialization in the area of auxiliary and portable power units and battery chargers.

They offer significant advantages over an external reformer based SOFC, namely, i simplicity in the overall system architecture and balance of plant, ii more efficient and iii availability of constant concentration of fuel in the anode compartment of SOFC providing stability factor.

The coking problem on the anode has been a serious and challenging issue faced by the catalyst research community worldwide. A careful investigation of variation in the microstructure and performance characteristics voltage-current curve and impedance of Ni and Cu-Ni anode before and after a long term exposure of CH4 and natural gas would allow us to test the validation of a. Electrochemical performance of 3D porous Ni-Co oxide with electrochemically exfoliated graphene for asymmetric supercapacitor applications.

Graphene sheets are directly obtained by an electrochemical exfoliation process with graphite foil, which is very simple, environmentally friendly, and has a relatively short reaction time. This electrochemically exfoliated graphene EEG can improve the electrical conductivity of the Ni-Co oxide nanostructures. The as-prepared NC-EEG nanocomposites have 3D porous architectures that can provide large surface areas and shorten electron diffusion pathways.

Electrochemical oxidation of nitrite on nanodiamond powder electrode. Chen, L. Nanodiamond ND powder electrodes were fabricated and the electrochemical properties were investigated in the solution containing nitrite in this article. This electrode exhibits substantial catalytic ability toward the oxidation of nitrite anions. The electrochemical oxidation mechanism of nitrite on the ND powder electrode is discussed.

The electrode reaction rate constant k is estimated to be 2. Oxidative electrochemical aryl C-C coupling of spiropyrans. The isolation and definitive assignment of the species formed upon electrochemical oxidation of nitro-spiropyran SP is reported. The oxidative aryl C-C coupling at the indoline moiety of the SP radical cation to form covalent dimers of the ring-closed SP form is demonstrated. The coupling is. Electrochemical Oxidation of Phenol using a Flow-through Micro The electrochemical oxidation of phenol to benzoquinone followed by the reduction to hydroquinone and catechol was demonstrated by constructing a three-dimensional porous micro-flow cell from lead dioxideand lead.

The electrodes were made by using the principles of curing and formation of lead oxide material that Method and electrochemical cell for synthesis and treatment of metal monolayer electrocatalysts metal, carbon, and oxide nanoparticles ion batch, or in continuous fashion.

An apparatus and method for synthesis and treatment of electrocatalyst particles in batch or continuous fashion is provided. In one embodiment, the apparatus comprises a sonication bath and a two-compartment chamber submerged in the sonication bath. The upper and lower compartments are separated by a microporous material surface. The upper compartment comprises a cover and a working electrode WE connected to a Pt foil contact, with the foil contact connected to the microporous material.

The upper chamber further comprises reference counter electrodes. The lower compartment comprises an electrochemical cell containing a solution of metal ions. In one embodiment, the method for synthesis of electrocatalysts comprises introducing a plurality of particles into the apparatus and applying sonication and an electrical potential to the microporous material connected to the WE.

After the non-noble metal ions are deposited onto the particles, the non-noble metal ions are displaced by noble-metal ions by galvanic displacement. Ammonia removal in electrochemical oxidation : Mechanism and pseudo-kinetics. The results show that the ammonia oxidation rates resulted from direct oxidation at electrode-liquid interfaces of the anode by stepwise dehydrogenation, and from indirect oxidation by hydroxyl radicals were so slow that their contribution to ammonia removal was negligible under the condition with Cl -.

The oxidation rates of ammonia ranged from 1. The removed one was subsequently found in the form of N 2 in the produced gas. The rate at which Cl - lost electrons at the anode was a major factor in the overall ammonia oxidation. The ammonia was reduced to less than 0. This result was in line with the strict discharge requirements. Nanomaterials-based electrochemical sensors for nitric oxide. Electrochemical sensing has been demonstrated to represent an efficient way to quantify nitric oxide NO in challenging physiological environments.

A sensing interface based on nanomaterials opens up new opportunities and broader prospects for electrochemical NO sensors. This review with refs. It is subdivided into sections on i carbon derived nanomaterials such as carbon nanotubes, graphenes, fullerenes , ii metal nanoparticles including gold, platinum and other metallic nanoparticles ; iii semiconductor metal oxide nanomaterials including the oxides of titanium, aluminum, iron, and ruthenium ; and finally iv nanocomposites such as those formed from carbon nanomaterials with nanoparticles of gold, platinum, NiO or TiO 2.

The various strategies are discussed, and the advances of using nanomaterials and the trends in NO sensor technology are outlooked in the final section. Effect of oxide ion concentration on the electrochemical oxidation of carbon in molten LiCl. The continuous measurement of lithium oxide concentration was required in DOR Direct Oxide Reduction process, which converts spent nuclear fuel to metal form, for the reactivity monitor and effective control of the process.

The concentration of lithium oxide was measured by the electrochemical method, which was based on the phenomenon that carbon atoms of glassy carbon electrode electrochemically react with oxygen ions of lithium oxide in molten LiCl medium. From the results of electrode polarization experiments, the trend of oxidation rate of carbon atoms was classified into two different regions, which were proportional and non-proportional ones, dependent on the amount of lithium oxide.

Below about 2. In this concentration range, the oxidation rate of carbon atoms was controlled by the diffusion of lithium oxide , and the concentration of lithium oxide could be measured by electrochemical method. But, above 2. Above this concentration, the electrochemical method was not applicable to determine the concentration of lithium oxide.

Kudr, J. Electrochemical oxidation of selective estrogen receptor modulator raloxifene. The oxidation mechanism of raloxifene with different pH values was studied by cyclic voltammetry, X-ray photoelectron spectroscopy XPS , in situ UV—vis spectral analysis and cyclic voltabsorptometry based on a long optical-path thin-layer electrochemical cell. Time-derivative cyclic voltabsorptograms were obtained for comparative discussion with the corresponding cyclic voltammograms.

Raloxifene was initially oxidized to reactive phenoxyl radicals, followed by a series of transformation steps leading to different final products in different pH media. A parallel-consecutive reaction mechanism was proposed for the pH-dependent formation of 7-hydroxyraloxifene, raloxifene 6,7-o-quinone and two raloxifene dimers, each pathway following a complex electrochemical -chemical mechanism. Both raloxifene diquinone methide and its N- oxides were not detected by in situ UV—vis spectroscopy and XPS analysis.

This work provides an electrochemical viewpoint and comparable information for better understanding of the oxidative metabolism and chemical toxicology of raloxifene under physiological conditions in vivo or in vitro. Electrochemical advanced oxidation processes: today and tomorrow. A review. In recent years, new advanced oxidation processes based on the electrochemical technology, the so-called electrochemical advanced oxidation processes EAOPs , have been developed for the prevention and remediation of environmental pollution, especially focusing on water streams.

This paper presents a general overview of the application of EAOPs on the removal of aqueous organic pollutants, first reviewing the most recent works and then looking to the future. A global perspective on the fundamentals and experimental setups is offered, and laboratory-scale and pilot-scale experiments are examined and discussed. Electrochemical oxidation of niclosamide at a glassy carbon Cyclic voltammetry, square-wave voltammetry and controlled potential electrolysis have been used to study the electrochemical oxidation behaviour of niclosamide at a glassy carbon electrode.

The number of electrons transferred, the wave characteristics, the diffusion coefficient and reversibility of the reactions have been Fractional surface termination of diamond by electrochemical oxidation. The crystalline form of sp 3 -hybridized carbon, diamond, offers various electrolyte-stable surface terminations. This is of particular interest for all applications relying on interfacial electrochemistry, especially for biointerfaces. Electrochemical reduction of actinides oxides in molten salts.

Reactive metals are currently produced from their oxide by multiple steps reduction techniques. A one step route from the oxide to the metal has been suggested for metallic titanium production by electrolysis in high temperature molten chloride salts. In the so-called FFC process, titanium oxide is electrochemically reduced at the cathode, generating O 2- ions, which are converted on a graphite anode into carbon oxide or dioxide.

After this process, the spent salt can in principle be reused for several batches which is particularly attractive for a nuclear application in terms of waste minimization. In this work, the electrochemical reduction process of cerium oxide IV is studied in CaCl 2 and CaCl 2 -KCl melts to understand the oxide reduction mechanism. Cerium is used as a chemical analogue of actinides. Electrolysis on 10 grams of cerium oxide are made to find optimal conditions for the conversion of actinides oxides into metals.

The scale-up to hundred grams of oxide is also discussed. Electrochemical preparation of new uranium oxide phases. Oxides UO and U 3 O 4 are thermodynamically unstable at low temperatures and decompose into uranium oxide of the composition UO 2-x , where x varies from 0 to 0.

Electrochemistry combined with mass spectrometry EC-MS is an emerging analytical technique in the imitation of oxidative drug metabolism at the early stages of new drug development. Here, we present the benefits of electrochemical oxidation by square-wave potential pulses for the oxidation of. Full Text Available FeCrAl is comprised essentially of Fe, Cr, Al and generally considered as metallic substrates for catalyst support because of its advantage in the high-temperature corrosion resistance, high mechanical strength, and ductility.

Oxidation film and its adhesion on FeCrAl surface with aluminum are important for catalyst life. In this research, PEO plasma electrolytic oxidation process was applied to form the aluminum oxide on FeCrAl surface, and the formed oxide particle according to process conditions such as electric energy and oxidation time were investigated. The study presents possibility of aluminum oxide formation by electro-chemical coating process without any pretreatment of FeCrAl.

Photocatalytic and electrochemical combined treatment of textile wash water. Various chemical and physical processes for treatment of textile effluent are not destructive but they only transfer the contaminants from one form to another. The presence of high concentration of organic dye and total dissolved solids TDS in the effluent that are not removed by biological treatment must be eliminated by an alternative method to the conventional ones is the advanced oxidation process AOP.

A procion blue dye effluent was treated by photo and electrochemical oxidation process as well as by combining photocatalytic degradation using TiO 2 suspensions. Chemical oxygen demand COD and colour removal can be used to follow the degradation of the organic pollutant.

The effects of pH, current density, flow rate of effluent that passes into the reactor and supporting electrolyte were studied. Comparative studies were carried out on photocatalytic and electrochemical process to degrade the procion blue. Integrating electrochemical oxidation into forward osmosis process for removal of trace antibiotics in wastewater.

During the rejection of trace pharmaceutical contaminants from wastewater by forward osmosis FO , disposal of the FO concentrate was still an unsolved issue. In this study, by integrating the advantages of forward osmosis and electrochemical oxidation , a forward osmosis process with the function of electrochemical oxidation FOwEO was established for the first time to achieve the aim of rejection of trace antibiotics from wastewater and treatment of the concentrate at the same time.

A synergetic effect between forward osmosis and electrochemical oxidation was observed in FOwEO, which lies in that antibiotic rejections by FO were enhanced due to the degradation of antibiotics in the concentrate, while the electrochemical oxidation capacity was improved in the FOwEO channel, of which good mass transfer and the assist of indirect oxidation owing to the reverse NaCl from draw solution were supposed to be the mechanism.

This study demonstrated that the FOwEO has the capability to thoroughly remove trace antibiotics from wastewater. Zinc oxide nanostructures for electrochemical cortisol biosensing. In this paper, we report on fabrication of a label free, highly sensitive and selective electrochemical cortisol immunosensors using one dimensional 1D ZnO nanorods ZnO-NRs and two dimensional nanoflakes ZnO-NFs as immobilizing matrix.

Anti-cortisol antibody Anti-Cab are used as primary capture antibodies to detect cortisol using electrochemical impedance spectroscopy EIS. The charge transfer resistance increases linearly with increase in cortisol concentration and exhibits a sensitivity of 3. M -1 for ZnO-NFs.

The observed sensing parameters are in physiological range. The developed sensors can be integrated with microfluidic system and miniaturized potentiostat to detect cortisol at point-of-care. Manganese oxide -based materials as electrochemical supercapacitor electrodes. Electrochemical supercapacitors ECs , characteristic of high power and reasonably high energy densities, have become a versatile solution to various emerging energy applications. This critical review describes some materials science aspects on manganese oxide -based materials for these applications, primarily including the strategic design and fabrication of these electrode materials.

Nanostructurization, chemical modification and incorporation with high surface area, conductive nanoarchitectures are the three major strategies in the development of high-performance manganese oxide -based electrodes for EC applications. Numerous works reviewed herein have shown enhanced electrochemical performance in the manganese oxide -based electrode materials. However, many fundamental questions remain unanswered, particularly with respect to characterization and understanding of electron transfer and atomic transport of the electrochemical interface processes within the manganese oxide -based electrodes.

In order to fully exploit the potential of manganese oxide -based electrode materials, an unambiguous appreciation of these basic questions and optimization of synthesis parameters and material properties are critical for the further development of EC devices references. Electrochemical investigations of ion-implanted oxide films.

Oxide films passive films of nm thickness were prepared by anodic polarization of hafnium and titanium electrodes up to 20 V. Multiple-energy ion implantation of palladium, iron and xenon was used in order to obtain modified films with constant concentration profiles of the implanted ions. Rutherford backscattering, X-ray photoelectron spectroscopy measurements and electrochemical charging curves prove the presence of implanted ions, but electrochemical and photoelectrochemical measurements indicate that the dominating effect of ion implantation is the disordering of the oxide film.

The capacity of hafnium electrodes increases as a result of an increase in the dielectric constant D. For titanium the Schottky-Mott analysis shows that ion implantation causes an increase in D and the donor concentration N. Additional electronic states in the band gap which are created by the implantation improve the conductivity of the semiconducting or insulating films.

This is seen in the enhancement of electron transfer reactions and its disappearance during repassivation and annealing. Energy changes in the band gap are derived from photoelectrochemical measurements; the absorption edge of hafnium oxide films decreases by approximately 2 eV because of ion implantation, but it stays almost constant for titanium oxide films. All changes in electrochemical behavior caused by ion implantation show little variation with the nature of the implanted ion.

Hence the dominating effect seems to be a disordering of the oxide. Progress in electrochemical synthesis of magnetic iron oxide nanoparticles. Recently, magnetic iron oxide particles have been emerged as significant nanomaterials due to its extensive range of application in various fields. In this regard, synthesis of iron oxide nanoparticles with desirable properties and high potential applications are greatly demanded. Therefore, investigation on different iron oxide phases and their magnetic properties along with various commonly used synthetic techniques are remarked and thoroughly described in this review.

Electrochemical synthesis as a newfound method with unique advantages is elaborated, followed by design approaches and key parameters to control the properties of the iron oxide nanoparticles. Additionally, since the dispersion of iron oxide nanoparticles is as important as its preparation, surface modification issue has been a serious challenge which is comprehensively discussed using different surfactants. Despite the advantages of the electrochemical synthesis method, this technique has been poorly studied and requires deep investigations on effectual parameters such as current density, pH, electrolyte concentration etc.

We report a simple electrochemical approach in fabricating multiple colored molybdenum Mo oxide bronzes on the surface of a Mo-quartz electrode. A three step electrochemical batch process consisting of linear sweep voltammetry and anodic oxidation followed by cathodic reduction in neutral K 2 SO 4 electrolyte at different end potentials, viz. The color variation was suggested to be associated with the cations intercalation into the oxide formed and the simultaneous structural changes that occurred during the cathodic reduction in neutral aqueous medium.

Destination of organic pollutants during electrochemical oxidation of biologically-pretreated dye wastewater using boron-doped diamond anode. Electrochemical oxidation of biologically-pretreated dye wastewater was performed in a boron-doped diamond BDD anode system. After electrolysis of 12h, the COD was decreased from to 99 mg L -1 destination of organic pollutants during electrochemical oxidation process was carefully investigated by molecular weight distribution measurement, resin fractionation, ultraviolet-visible spectroscopy, HPLC and GC-MS analysis, and toxicity test.

As results, most organic pollutants were completely removed by electrochemical oxidation and the rest was primarily degraded to simpler compounds e. Especially, the performance of BDD anode system in degradation of large molecular organics such as humic substances makes it very promising in practical applications as an advanced treatment of biologically-pretreated wastewaters. More importantly, the destination of organic pollutants during electrochemical oxidation process was carefully investigated by molecular weight distribution measurement, resin fractionation, ultraviolet-visible spectroscopy, HPLC and GC-MS analysis, and toxicity test.

We show that materials which bind oxygen intermediates We present a rational design principle for the selectivity in electrochemical water oxidation and identify new material candidates that could perform H2O2 evolution selectively Full Text Available Typically, anodic oxidation of metals results in the formation of hexagonally arranged nanoporous or nanotubular oxide , with a specific oxidation state of the transition metal.

Recently, the majority of transition metals have been anodized; however, the formation of copper oxides by electrochemical oxidation is yet unexplored and offers numerous, unique properties and applications. Nanowires formed by copper electrochemical oxidation are crystalline and composed of cuprous CuO or cupric oxide Cu2O, bringing varied physical and chemical properties to the nanostructured morphology and different band gaps: 1.

According to its Pourbaix potential-pH diagram, the passivity of copper occurs at ambient and alkaline pH. To date, no systemic study has yet been reported on the influence of the operating conditions, such as the type of electrolyte, its temperature, and applied potential, on the morphology of the grown nanostructures.

However, the numerous reports gathered in this paper will provide a certain view on the matter. After passivation, the formed nanostructures can be also post-treated. Post- treatments employ calcinations or chemical reactions, including the chemical reduction of the grown oxides.

Nanostructures made of CuO or Cu2O have a broad range of potential applications. On one hand, with the use of surface morphology, the wetting contact angle is tuned. On the other hand, the chemical composition pure Cu2O and high surface area make such materials attractive for renewable energy harvesting, including water splitting.

While compared to other fabrication techniques, self-organized anodization is a facile, easy to scale-up, time-efficient approach, providing high-aspect ratio one-dimensional 1D nanostructures. Despite these advantages, there are still numerous challenges that have to be faced, including the. Preparation of the electrochemically formed spinel-lithium manganese oxides.

Electrochemically formed spinel-lithium manganese oxides were synthesized from manganese hydroxides prepared by a cathodic electrochemical precipitation from various concentrations of manganese nitrate solutions. Electrochemical studies on vanadium oxides , 9. It was shown that all the organics were oxidized by the so called hole-current doubling mechanism, and that the oxygen evolution reaction, which competed with the above oxidation reaction at the hole-capturing step from the valence band of the electrode, proceeded by the simple hole-capturing mechanism, not followed by an electron injection step into the conduction band.

Furthermore, it is considered that chloride ions added to the electrolytes tended to hinder hole-current doubling oxidation owing to their reactivity with the holes at the illuminated V 2 O 5 electrodes. Application of molybdenum and phosphate modified kaolin in electrochemical treatment of paper mill wastewater.

Pulp and paper mill wastewater is characterized by very high chemical oxygen demand COD values that inhibit the activity of microorganisms during biological oxidations. The electrochemical degradation of pulp and paper mill wastewater catalyzed by molybdenum and phosphate Mo-P modified kaolin with graphite as anode and cathode was investigated. A possible mechanism for degradation of the mill wastewater constituents was also proposed. Electrochemical oxidation of biological pretreated and membrane separated landfill leachate concentrates on boron doped diamond anode.

Zhou, Bo, E-mail: qq. The electrochemical oxidation of landfill leachate concentrates from disc tube reverse osmosis DTRO process over a BDD anode was investigated. The instantaneous current efficiency ICE was used to appraise different operating conditions. Under these conditions, Electrochemical synthesis and characterization of copper I oxide.

Full Text Available The quest and need for clean and economical energy sources have increased interest in the development of thin film cells technologies. Electrochemical deposition is an attractive method for synthesis of thin films.

It offers the advantages of low synthesis temperature, low cost and high purity. Copper I oxide or cuprous oxide is an oxide semiconductor which is used as the anodic material in the form of thin film in lithium batteries and solar cells. The cathodic process of synthesis of cuprous oxide thin film is carried out in a potentiostatic mode from the organic electrolyte. The process parameters are chosen in that way to accomplish maximum difference between the potentials at which Cu2O and CuO are obtained.

The electrochemical characterization was carried out by cyclic voltammetry. The electrodeposition techniques are particularly well suited for the deposition of single elements but it is also possible to carry out simultaneous depositions of several elements and syntheses of well-defined alternating layers of metals and oxides with thicknesses down to a few nm.

Nanomaterials exhibit novel physical properties and play an important role in fundamental research. In addition, cuprous oxide is commonly used as a pigment, a fungicide, and an antifouling agent for marine paints.

It is insoluble in water and organic solvents. This work presents the examinations of the influence of bath, temperature, pH and current density on the characteristics of electrochemically synthesized cuprous oxide. In the 'classic' process of synthesis, which is carried out under galvanostatic conditions on the anode, the grain size of the powder decreases with the increase in current density while the grain colour becomes lighter.

Electrochemical oxidation of textile industry wastewater by graphite electrodes. In the present article, studies have been performed on the electrochemical EC oxidation of actual textile industry wastewater by graphite electrodes. Multi-response optimization of four independent parameters namely initial pH pHo : , current density j : It was aimed to simultaneously maximize the chemical oxygen demand COD and color removal efficiencies and minimize specific energy consumption using desirability function approach.

Maximum COD and color removal and minimum specific energy consumed was The wastewater, sludge and scum obtained after treatment at optimum condition have been characterized by various techniques. UV-visible study showed that all azo bonds of the dyes present in the wastewater were totally broken and most of the aromatic rings were mineralized during EC oxidation with graphite electrode. Carbon balance showed that out of the total carbon eroded from the graphite electrodes, Nitrogen-doped reduced graphene oxide electrodes for electrochemical supercapacitors.

Building on a previous work detailing the synthesis of this material, electrodes were fabricated via spray-deposition of aqueous dispersions and the electrochemical charge storage mechanism was investigated. Results indicate that the functionalised graphene displays improved performance compared to non-functionalised graphene. The simplicity of fabrication suggests ease of up-scaling of such electrodes for commercial applications.

An overview on the removal of synthetic dyes from water by electrochemical advanced oxidation processes. Wastewater containing dyes are one of the major threats to our environment. Conventional methods are insufficient for the removal of these persistent organic pollutants. Recently much attention has been received for the oxidative removal of various organic pollutants by electrochemically generated hydroxyl radical. This review article aims to provide the recent trends in the field of various Electrochemical Advanced Oxidation Processes EAOPs used for removing dyes from water medium.

The characteristics, fundamentals and recent advances in each processes namely anodic oxidation , electro-Fenton, peroxicoagulation, fered Fenton, anodic Fenton, photoelectro-Fenton, sonoelectro-Fenton, bioelectro-Fenton etc. These processes have great potential to destroy persistent organic pollutants in aqueous medium and most of the studies reported complete removal of dyes from water. The great capacity of these processes indicates that EAOPs constitute a promising technology for the treatment of the dye contaminated effluents.

Sulfur tolerant composite cermet electrodes for solid oxide electrochemical cells. An electrochemical apparatus is made containing an exterior electrode bonded to the exterior of a tubular, solid, oxygen ion conducting electrolyte where the electrolyte is also in contact with an interior electrode, said exterior electrode comprising particles of an electronic conductor contacting the electrolyte, where a ceramic metal oxide coating partially surrounds the particles and is bonded to the electrolyte, and where a coating of an ionic-electronic conductive material is attached to the ceramic metal oxide coating and to the exposed portions of the particles.

Writing nanopatterns with electrochemical oxidation on redox responsive organometallic multilayers by AFM.

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A supportive class and baseball enthusiast at heart, Rudy spends his time healing his fellow party members, casting defensive spells, pitching near-perfect games, and listening to video game music. Gamer Since: Fire Serpent Another notable AK skin. Log in or register to post comments. More Top Stories. It features a granite-like background color with dark spots resembling stains all over the body.

One of the best parts of the game is the vast amount of different skins you can get. To explain it quickly, unlike other games where you buy skins outright, in CSGO the easiest way to get skins It tells you where your bullets are headed, and where they are going to land. No matter what is happening in a match, your crosshair will The handle is a light brown color with a shiny silver top that just completes the look.

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Knives are one of, if not the most iconic weapon featured in CS:GO. Without further to do, here are the top 15 knife skins currently in CS:GO. Centered around weapon skins of varying rarity that players receive Sensitivity is the most crucial parts of any CSGO players performance. It is how fast your pointer moves across the screen, or how slow it is. Higher sensitivities mean there is less effort needed to move your pointer from one side to the other. The other end is a low sensitivity, meaning the One reason why some players are better than others is the amount of time spent on practice and on learning specific map tactics.

In this article I will be covering mainly which maps are the best to practice against your friends. Practicing on 1v1 maps is very beneficial especially against The pocket AWP. The one tap. The Juan deag. In the right hands, the deagle is arguably the deadliest pistol in CS:GO.

If you plan to use one, why not go out with a bang? Using a traditional style of Japanese painting, the Midnight Storm features a teal The number of bullets, recoil as well as damage will determine how many enemies you destroy each round. Looking for a new knife skin? Well you best check your bank account because this list of the best knife skins doesn't come cheap! That being said, these skins are still pretty awesome! Bayonet Night Although like the M9 Bayonet, this skin poses a narrower blade with a straight How do you know what to open?

While buying and trading directly with other players might be the most cost-effective way of getting the skins you want, cases not only offer you a chance at rare skins for a fraction of the cost but opening They make the game look easy. They come through when their team needs them the most. Allow me to introduce the top 10 CS:GO players in Twistzz Currently boasts one of the highest headshot percentages in Russel Van Dulken is a 21 year-old Canadian Streaming has been a huge part of game industry since Besides playing professionally, many players have chosen to broadcast their gameplay on Twitch.

Shroud Mike " Well, welcome to the club. Over the years thousands of community training maps have been created and only a few have stood the test of time. The M4A Description: It has individual parts spray-painted black and tangerine orange. Flavor Text: Rona is as good as she thinks she is Killing enemies in shooter games is bread and butter.

However, doing so in CS:GO requires certain amount of skill and knowledge. Knowing when to peek and shoot is often more important than having good aim. Here, we present some of the best tips on becoming a killing spree machine Wondering who is considered the best AWPers in the world currently?

Look no further as these players are currently deemed to be among the top 10 best in the world. Voted the 20th best player of Skins can be a fickle thing in Counter-Strike. Many players enjoy admiring and flaunting expensive skins, but not all of us have the means or the will to invest that much into a digital luxury.

Luckily not all skins are expensive, and not all good looking skins are expensive, and what XM Who needs aim anyway? Yes, the Benelli M4 Super 90 boasts the highest fire-rate of all shotguns with 7 shots before reload. Under the right The year was exciting. With many big tournaments, players had the opportunity to prove themselves as true winners.

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